Witryna15 sty 2024 · Based on previously reported data, it was determined that C-2 of impurity 1 was in the S configuration ( Van Heyningen and Ahern, 1968 ). In the enhanced mass spectrum (positive ion mode) of impurity 2, peaks were identified at m/z 526.3 ( [M+H] +) and 548.3 ( [M+Na] + ). Witrynaimpurities, containers, sample preparation devices, volatile organics introduced as a result of handling personal care products, and even columns themselves. Plasticizers from labware can interfere with LC-MS, resulting in the need to lengthen the chromatography run in order to resolve these peaks from analyte peaks.
Cyclotron-based production of 68Ga, [68Ga]GaCl3, and
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